Hach-lange BIOGAS User Manual Manuel d'utilisateur

DOC022.52.90424BIOGAS Titration Manager08/2012, Edition 1AUser Manual© HACH Company, 2012. All rights reserved. Printed in France.

10Installation3.4 InterfacesFigure 2 Interfaces3.5 Installation of burettes and reagentsRefer to:• BIOGAS Titration Manager Installation form, Catalog

11Installation

12Kapitel 4 Startup4.1 Power the instrument on and off1. Connect the power cable to a power socket.2. Switch on the instrument via the power switch on

13Startup

14Kapitel 5 Standard Operations5.1 OverviewThe interface of the BIOGAS Titration Manager has been specially designed to clearly guide you through ever

15Standard Operations5.1.2 General screen descriptionFigure 4 General screen description:Note: The UP and DOWN keys allow you to select a line. To ent

16Standard Operations5.2 Main menuWhen the instrument is switched on the Main window is displayed.Figure 5 Main menu5.3 Reagent menuPress the RIGHT ar

17Standard OperationsFigure 6 Reagents menu1 Title bar: indicates the name of the window.5GLP-Archives: access GLP tables and visualise the last reage

18Standard Operations5.4 Electrode menuPress twice the RIGHT arrow key in the Main menu to move to the Electrode menu.Figure 7 Electrode menu1 Title b

19Standard Operations5.5 Cell menuPress three times the RIGHT arrow key in the Main menu to move to the Electrode menu.Figure 8 Cell menuApply interna

2Table of contentsSection 1 Specifications... 4Section 2

20Standard Operations3. Adjust stirring by turning the stirring propeller knob. Note: You can consult the corresponding table between the position (1

21Standard Operations2. Press the RIGHT arrow key to move to the next screen in the Configuration menu.3. Press the UP arrow key to scroll in the Conf

22Standard Operations5.6.1.1 Date and time1. Select Time in the Configuration menu.2. Enter the hours (from 00 to 23).3. Press the RIGHT arrow key.4.

23Standard Operations12. Press the RIGHT arrow key.13. Enter the year (from 2000 to 2069).14. Press the validation key (as indicated on the screen).5.

24Standard Operations9. Enter the text using the PC keyboard (maximum of 32 characters can be used). Note: If the characters shown on the display do n

25Standard Operations4. To correct a typing error, proceed as follows: a. Press the LEFT arrow key to position the cursor on the letter "E".

26Standard Operationspage 23). This information will appear as a header at the start of the printout. 8. For automatic printout - select a condensed o

27Standard OperationsFigure 12 Method data5.8.2 Edit reagent data1. Press 5 Reagent library in the Reagent menu.2. Press 2 to access. These are the pa

28Standard Operations2. Press 2 to access. These are the parameters entered in the Edit electrode screen. 3. Press Print to get an overview of the pa

29Standard OperationsFigure 13 Example of a printout for a titration5.9 Store, send and recall data5.9.1 The data logThe last 60 results are saved in

3Table of contents5.11 Run analyses...425.11.1

30Standard OperationsExamples:Result no. 1/9 = Mean and standard deviationMean and standard deviation calculated on "TAC" test results.Resul

31Standard OperationsResult no. 1/9 = Mean and standard deviationMean and standard deviation calculated on "FOS" test results.Result no. 1/9

32Standard OperationsResult no. 2/9 = Test no.1"Volume A" result for test no.1.Result no. 2/9 = Test no.1"Volume B" result for tes

33Standard OperationsResult no. 2/9 = Test no.1"FOS/TAC" result for test no.1.5.9.2 The reagent calibration logThe last performed (current)

34Standard Operations5.10 Program instructionsNote: Only the Supervisor is allowed to program the menus, Electrode, Reagent, and Method.To select the

35Standard Operations2. Press 1 (New electrode).3. Press the validation key in the Function field4. Select the function of the electrode, refer to the

36Standard OperationsNote: When a combined electrode has been defined, the instrument will prompt you to specify if it has a built-in temperature sens

37Standard Operations5.10.1.1 Edit an electrode1. Enter the Electrode menu and press 4 (Electrode library).2. Press the validation key and select the

38Standard Operations5.10.1.2 Enter the electrode parameters1. Select Calibrate request = yes2. Enter the electrode definition parameters3. Go to the

39Standard Operations5.10.2.1 Edit a reagent1. Enter the Reagent menu and press 5 (Reagent library).2. Press the validation key and select the reagent

4Section 1 SpecificationsSpecifications are subject to change without notice.MethodsEnd point titration 1 to 3 pre-setInflection point titrationAuto d

40Standard Operations5.10.2.2 Enter the reagent parameters1. Select Titre = Calibrate2. Enter the Edit reagent menu and press 1 (Calibration parameter

41Standard Operations5.10.3.1 Edit a method1. Enter the Method menu and press 5 (Method library).2. Press the validation key and select the method to

42Standard Operations10. Select Blank: A blank or blank sample is usually a solvent used to dissolve or dilute the sample. This blank may contain trac

43Standard OperationsIdentify electrodes (including temperature sensors) to be used for the analysis. Electrodes can be created from the following lis

44Standard OperationsNote: When Cloudy/Stormy/Question mark icons appear, Press 1 Check. The Titration Manager will automatically guide you through th

45Standard Operations1. Press 2 (Select method) in the main menu.If Question marks "?" are present in the electrode and/or reagent tabs. Pro

46Standard Operations6. Press the validation key.7. Select the reagent from the proposed list. 8. Press 1 to start the calibration.5.11.4 Run a metho

47Standard Operations

48Section 6 Maintenance6.1 Cleaning the instrumentThe BIOGAS Titration Manager requires minimum maintenance. The exterior surface can be cleaned with

49

5SpecificationsBurette1 embedded burette standBurette volumes available 1, 5, 10, 25, 50 mLBurette motor 18000 stepsComplies with ISO/FDIS 8655-3UV-pr

50Section 7 Troubleshooting7.1 TroubleshootingIf you have forgotten an operation while editing the method, icons visible in the Electrode and Reagent

51

52Section 8 Replacement Parts and Accessories8.1 Burette standsCat. NumberB505 Burette Stand, 5 mL, UV protected with connection tubing X51T026B510 Bu

53Replacement Parts and Accessories8.7 Electrode Maintenance SolutionsCat. NumberRENOVO N - Normal Cleaning Solution, 250 mL S16M001RENOVO X - Xtra St

54Section 9 Contact InformationHACH CompanyWorld HeadquartersP.O. Box 389Loveland, Colorado80539-0389 U.S.A.Tel (800) 227-HACH(800) -227-4224(U.S.A. o

55Contact InformationHACH LANGE KFT.Vöröskereszt utca. 8-10.H-1222 Budapest XXII. ker.Tel. +36 1 225 7783Fax +36 1 225 [email protected]

6Section 2 General Information2.1 Safety notesPlease read this entire manual before unpacking, setting up, or operating this equipment. Pay attention

7General Information2.1.3 Chemical and Biological SafetyNormal operation of this device may require the use of chemicals or samples that are biologica

8Section 3 Installation3.1 Unpacking the instrumentsThe BIOGAS Titration Manager comes packaged with the following items:• BIOGAS Titration Manager, o

9Installation3.3 Power connectionsFigure 1 Power connection1. Plug the power cable into the back of the instrument (Figure 1).2. Insert the plug of th